Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetophenone → 4,4'-methylenebis{N-(alpha-methylbenzylidene)aniline}
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetophenone | HCID 7410 | — |
| 반응물 | 4,4-Diaminodiphenylmethane | HCID 7577 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 4,4'-methylenebis{N-(alpha-methylbenzylidene)aniline} | HCID 21388895 | — |
반응 단계
A mixture of 4,4'-methylene dianiline (198 g; 1 mole), acetophenone (240 g; 2 moles) and a catalytic amount of stannous chloride was refluxed in toluene (3L) for 30 hours using a Dean-Stark trap. The theoretical amount of water was removed from the system. The toluene was then removed under vacuum.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03944525 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-4c305abc2c81423a93ea19c9f6858e66 |
| 출처 메모 | uspto-grants-1976_03 |