Ethamivan → p-geranyloxy-m-methoxy-N,N-diethyl-benzamide

HRID 267714노트

반응식

HRID 267714 반응식
[CH2:1](Br)/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4].[CH2:12]([N:14]([CH2:26][CH3:27])[C:15](=[O:25])[C:16]1[CH:24]=[CH:23][C:21]([OH:22])=[C:18]([O:19][CH3:20])[CH:17]=1)[CH3:13]>>[CH2:1]([O:22][C:21]1[CH:23]=[CH:24][C:16]([C:15]([N:14]([CH2:26][CH3:27])[CH2:12][CH3:13])=[O:25])=[CH:17][C:18]=1[O:19][CH3:20])/[CH:2]=[C:3](/[CH2:5][CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])\[CH3:4]

참가 물질

3

반응물 2

HCID 9363EthamivanHCID 53658672,6-Octadiene, 1-bromo-3,7-dimethyl-, (2E)-

생성물 1

HCID 21487569p-geranyloxy-m-methoxy-N,N-diethyl-benzamide

실험 절차

geranyl bromide was reacted with vanillic acid N,N-diethyl amide to obtain p-geranyloxy-m-methoxy-N,N-diethyl-benzamide (boiling point = 180°/0.05 mmHg);

출처 및 근거

ORD 기록
ord-24c2b76e2c3e485fb245b4f3bcdf40d6
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03944531

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