HCID 68147811, 화합물 → HCID 21553917, 화합물

HRID 267782노트

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HRID 267782 반응식
[CH:1]([N:4]1[CH2:8][C:7]2([CH2:14][O:13][C:12]3[CH:15]=[CH:16][C:17]([NH:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])=[CH:18][C:11]=3[O:10][CH2:9]2)[O:6]C1=O)([CH3:3])[CH3:2]>C(O)C>[OH:6][C:7]1([CH2:8][NH:4][CH:1]([CH3:2])[CH3:3])[CH2:14][O:13][C:12]2[CH:15]=[CH:16][C:17]([NH:19][C:20]([O:22][CH2:23][CH3:24])=[O:21])=[CH:18][C:11]=2[O:10][CH2:9]1

참가 물질

3

반응물 1

HCID 68147811HCID 68147811, 화합물

생성물 1

HCID 21553917HCID 21553917, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

This oxazolidinone from Step A above is refluxed in ethanol containing anhydrous hydrogen chloride. The solution is neutralized, evaporated to a small volume, diluted with water and extracted with ether. The dried etheral solution is evaporated to give the desired product.

후처리

  1. customevaporated to a small volume
  2. additiondiluted with water
  3. extractionextracted with ether
  4. customThe dried etheral solution is evaporated

출처 및 근거

ORD 기록
ord-c6776d48462e4869873a3c58f3c6686b
출처 데이터셋
uspto-grants-1976_03
특허 번호
US03944560

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