Phenoxazine → 10-[1-(1-Pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

반응식

[CH:1]1[C:14]2[NH:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[O:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.Cl.[Cl:16][C:17]1[N:18]([C:22]2[CH2:26][CH2:25][CH2:24][N:23]=2)[CH2:19][CH2:20][CH:21]=1>>[ClH:16].[N:23]1[CH2:24][CH2:25][CH2:26][C:22]=1[N:18]1[CH2:19][CH2:20][CH:21]=[C:17]1[N:13]1[C:14]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=2[O:6][C:7]2[C:12]1=[CH:11][CH:10]=[CH:9][CH:8]=2

참가 물질

반응물 2

HCID 67278Phenoxazine

HCID 203071382-Chloro-1-(1-pyrrolin-2-yl) 2-pyrroline hydrochloride

생성물 1

HCID 2030714610-[1-(1-Pyrrolin-2-YL)-2-pyrrolin-2-YL]phenoxazine hydrochloride

실험 절차

Reaction of phenoxazine with 2-chloro-1-(1-pyrrolin-2-yl)pyrroline hydrochloride according to the procedure of Example 7 affords 10-[1-(1-PYRROLIN-2-YL)-2-PYRROLIN-2-YL]PHENOXAZINE HYDROCHLORIDE, m.p. 257.5°-263° C. (corr.), from ethanol-ether.

출처 및 근거

ORD 기록: ord-b52c13933b614eb88bdcb5d80273dd2e
출처 데이터셋: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03946004

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