Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2-Ethyl-6-methylaniline | HCID 32485 | — |
| 반응물 | 2-(Chloromethyl)-1,3-dioxolane | HCID 75727 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline | HCID 21435679 | — |
반응 단계
2-Ethyl-6-methylaniline (70 grams), 2-chloromethyl-1,3-dioxolane (30 grams), potassium carbonate (38 grams) and dimethylformamide (50 ml) were charged into a glass reaction vessel equipped with a mechanical stirrer, thermometer and reflux condenser. The reaction mixture was heated at reflux for a period of about 24 hours. After this time the mixture was filtered and distilled to yield the desired product N-(1,3-dioxolan-2-ylmethyl)-2-ethyl-6-methylaniline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03946044 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-f766387d9da6484f9e3a7c4a6a0b5b59 |
| 출처 메모 | uspto-grants-1976_03 |