Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Ethylhexanol → Toluene 2,4-Diisocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Ethylhexanol | HCID 7720 | — |
| 반응물 | Toluene 2,4-Diisocyanate | HCID 11443 | — |
| 반응물 | 2-Hexanone | HCID 11583 | — |
| 생성물 | Toluene 2,4-Diisocyanate | HCID 11443 | — |
| 생성물 | 2-Ethylhexanol monourethane | HCID 87961684 | — |
반응 단계
A 2-ethylhexanol monourethane of 2,4-toluene diisocyanate sample was prepared by adding 651 parts of 2-ethylhexanol to an agitated mixture of 870 parts of 2,4-TDI and 100 parts methyl butyl ketone over approximately 3 hours, with external cooling to maintain the reaction temperature below 18° C. After addition was complete, the batch was agitated an additional 2 hours and stored under dry nitrogen for subsequent use.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947339 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-915385be45e84c168c5487d71f9cf3c5 |
| 출처 메모 | uspto-grants-1976_03 |