Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butanal → Butanal
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butanal | HCID 261 | — |
| 반응물 | 1-Amino-3,3,5-trimethylcyclohexyl hydroperoxide | HCID 21510183 | — |
| 생성물 | Butanal | HCID 261 | — |
| 생성물 | 3,3,5-Trimethylcyclohexanone | HCID 13398 | — |
반응 단계
Butyraldehyde (28.8 g.) in petrol (100 c.c.) was cooled to below 0° and with stirring treated with 1-amino-1-hydroperoxy-3,3,5-trimethylcyclohexane (33 g.; 93% pure). When the solid had dissolved the aqueous phase was removed and the petrol solution dried with magnesium sulphate overnight at 0°. The working up as in Example 4 gave butyraldehyde, dihydroisophorone and the same peroxide (33.0 g.) b.p. 96° - 98°/0.6 mm. as in Example 4.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947406 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-56f3721040364bc79a96fcdf882b5025 |
| 출처 메모 | uspto-grants-1976_03 |