Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Butanal → Butanal
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Butanal | HCID 261 | — |
| 반응물 | Ammonia acetate | HCID 12432 | — |
| 반응물 | 1-Aminocyclohexyl hydroperoxide | HCID 19380058 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Butanal | HCID 261 | — |
| 생성물 | Cyclohexanone | HCID 7967 | — |
반응 단계
1-Aminocyclohexyl hydroperoxide (13.1 g.), butyraldehyde (7.2 g.), methanol (25 cc.) and ammonia acetate (1.0 g.) were mixed and stored at 0°C overnight. Working up as in Example 39 gave cyclohexanone and butyraldehyde, and a product (8.4 g.), b.p. 89°/0.3 mm. (peroxide equivalent, 204; pechloric acid equivalent, 206; which was identified as ##SPC37##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947406 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-d71560725e124bf9937c2ce881b6cce1 |
| 출처 메모 | uspto-grants-1976_03 |