Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formaldehyde → (3,4-dihydro-2(1H)-isoquinolinylmethyl]-1H-benz[de]isoquinoline-1,3(2H)-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | 1,2,3,4-Tetrahydroisoquinoline | HCID 7046 | — |
| 반응물 | Naphthalimide | HCID 66491 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | (3,4-dihydro-2(1H)-isoquinolinylmethyl]-1H-benz[de]isoquinoline-1,3(2H)-dione | HCID 21551797 | — |
반응 단계
An equimolar mixture of 1,2,3,4-tetrahydroisoquinoline, aqueous formaldehyde, and 1,8-naphthalimide is suspended in a small amount of dimethylformamide and the mixture is heated until dissolution is complete. The solution is allowed to stand at room temperature and the resulting precipitate is filtered off and dried to yield 2-[(3,4-dihydro-2(1H)-isoquinolinylmethyl]-1H-benz[de]isoquinoline-1,3(2H)-dione.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947452 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-86ae842f9f6b4d99be980a88a6d2904a |
| 출처 메모 | uspto-grants-1976_03 |