2-Phenyl-benzofuran → 3-[2-(2-Diethylaminoethoxy)benzoyl]-2-phenylbenzofuran

반응식

[C:1]1([C:7]2[O:8][C:9]3[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=3[CH:11]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl.[CH2:17]([N:19]([CH2:32][CH3:33])[CH2:20][CH2:21][O:22][C:23]1[CH:31]=[CH:30][CH:29]=[CH:28][C:24]=1[C:25](Cl)=[O:26])[CH3:18]>>[CH2:32]([N:19]([CH2:17][CH3:18])[CH2:20][CH2:21][O:22][C:23]1[CH:31]=[CH:30][CH:29]=[CH:28][C:24]=1[C:25]([C:11]1[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[O:8][C:7]=1[C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:26])[CH3:33]

참가 물질

반응물 2

HCID 35179362-Phenyl-benzofuran

HCID 214352662-(2-Diethylaminoethoxy)benzoyl chloride hydrochloride

생성물 1

HCID 214353133-[2-(2-Diethylaminoethoxy)benzoyl]-2-phenylbenzofuran

실험 절차

Acylation of 2-phenylbenzofuran with 2-(2-diethylaminoethoxy)benzoyl chloride hydrochloride by the procedure described in Example 6 gives the title compound.

출처 및 근거

ORD 기록: ord-d8d9f5f6c2ff459e970ba0968e4b8f19
출처 데이터셋: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03947470

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