Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-Methoxy-3-methylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4-Methoxy-3-methylbenzoic Acid | HCID 2759583 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4-Methoxy-3-methylbenzoyl chloride | HCID 21092930 | — |
반응 단계
A solution of 11.5 g. (0.07 mol.) of 3-methyl-4-methoxybenzoic acid and 10.7 g. (0.09 mol.) of thionyl chloride in 60 ml. of methylene chloride is refluxed on a steam bath for two hours. Concentration under reduced pressure and distillation of the residue gives 3-methyl-4-methoxybenzoic acid chloride, m.p. 37°-39°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947470 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-825962360d5b436aa0ad301d11e764e5 |
| 출처 메모 | uspto-grants-1976_03 |