Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyl formate → 3-(2'-Methyl-2'-formylaminobutyl)-indole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyl formate | HCID 74626 | — |
| 반응물 | 3-(2'-Amino-2'-methylbutyl)-indole | HCID 21552235 | — |
| 생성물 | 3-(2'-Methyl-2'-formylaminobutyl)-indole | HCID 21552229 | — |
반응 단계
The 3-(2'-methyl-2'-aminobutyl)-indole obtained as reduction product in accordance with Example 1 or 3 was reacted with phenyl formate to yield 3-(2'-methyl-2'-formylaminobutyl)-indole; melting point 121.5°-124.5°C. (from ether). Reduction thereof with LiAlH4 yielded 3-(2'-methyl-2'-methylaminobutyl)-indole having a melting point of 100°-103°C. (from cyclohexane).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03947584 |
| 출처 데이터셋 | uspto-grants-1976_03 |
| ORD ID | ord-8f956a4918304bc2a1e7c1de3a525c8b |
| 출처 메모 | uspto-grants-1976_03 |