N-3-Bromopropylphthalimide → 3-(3-Aminopropylamino)-1,2,4-thiadiazole

HRID 26893

반응식

HRID 26893 반응식
[NH2:1][C:2]1[N:6]=[CH:5][S:4][N:3]=1.C1(=O)[N:11](CCCBr)[C:10](=O)[C:9]2=CC=CC=[C:8]12>>[NH2:11][CH2:10][CH2:9][CH2:8][NH:1][C:2]1[N:6]=[CH:5][S:4][N:3]=1

참가 물질

3

반응물 2

HCID 21611N-3-BromopropylphthalimideHCID 202496641,2,4-Thiadiazol-3-amine

생성물 1

HCID 205576553-(3-Aminopropylamino)-1,2,4-thiadiazole

실험 절차

Reaction of 3-amino-1,2,4-thiadiazole with 3-phthalimidopropyl bromide and hydrazinolysis of the product gives 3-(3-aminopropylamino)-1,2,4-thiadiazole and from this intermediate N-methyl-N'-[3-(3-1,2,4-thiadiazolyl)-amino)propyl]thiourea is prepared.

출처 및 근거

ORD 기록
ord-e445b676276b45818555a8432fe40614
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04151288

연결된 노트

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