Dimethylamine → 4-Bromo-N,N-dimethylbenzenesulphonamide

반응식

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH3:12][NH:13][CH3:14]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([N:13]([CH3:14])[CH3:12])(=[O:10])=[O:9])=[CH:4][CH:3]=1

참가 물질

반응물 2

HCID 674Dimethylamine

HCID 7396p-Bromobenzenesulfonyl chloride

생성물 1

HCID 128184-Bromo-N,N-dimethylbenzenesulphonamide수율 77%

실험 절차

Prepared by general procedure III from 4-bromobenzenesulfonyl chloride (9.59 g, 38 mmol) and excess aq. dimethylamine to give the title compound (7.61 g, 77%) as a white crystalline solid. MS (ISP) 266.1[(M+H)+].

출처 및 근거

ORD 기록: ord-492a9d2e985445f196e5384122d685f0
출처 데이터셋: uspto-grants-2008_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07446113B2

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