Ethanolamine → 4-bromo-N-(2-hydroxyethyl)benzenesulfonamide

HRID 268951노트

반응식

HRID 268951 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8](Cl)(=[O:10])=[O:9])=[CH:4][CH:3]=1.[CH2:12]([CH2:14][NH2:15])[OH:13]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:15][CH2:14][CH2:12][OH:13])(=[O:10])=[O:9])=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 700EthanolamineHCID 7396p-Bromobenzenesulfonyl chloride

생성물 1

HCID 4585694-bromo-N-(2-hydroxyethyl)benzenesulfonamide수율 98%

실험 절차

Prepared by general procedure III from 4-bromobenzenesulfonyl chloride (5.0 g, 20 mmol) and ethanolamine (1.32 g, 22 mmol) to give the title compound (5.4 g, 98%) as an off-white solid. MS (ISP) 280.0[(M+H)+].

출처 및 근거

ORD 기록
ord-da020de796e04b76ace07af57f94c903
출처 데이터셋
uspto-grants-2008_11
특허 번호
US07446113B2

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