Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenethylamine → N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenethylamine | HCID 1001 | — |
| 반응물 | 2-(2-Morpholinoethoxy)benzaldehyde | HCID 976593 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine | HCID 21322775 | 85.6% |
반응 단계
2-[2-(4-Morpholinyl)ethoxy]benzaldehyde (55.9 g) is reacted with 29 g of phenethylamine in 240 ml of toluene following the procedure described in Example 1A to yield 68.8 g of product as an oil, boiling point 204°-210° C. at 0.1-0.2 mm of Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04151354 |
| 출처 데이터셋 | uspto-grants-1979_04 |
| ORD ID | ord-4ac30af58cde4ba28f2ed7a5aea79b00 |
| 출처 메모 | uspto-grants-1979_04 |