Phenethylamine → N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine

HRID 26966

반응식

HRID 26966 반응식
[N:1]1([CH2:7][CH2:8][O:9][C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[CH:12]=O)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[CH2:18]([NH2:26])[CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>C1(C)C=CC=CC=1>[N:1]1([CH2:7][CH2:8][O:9][C:10]2[CH:17]=[CH:16][CH:15]=[CH:14][C:11]=2[CH:12]=[N:26][CH2:18][CH2:19][C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

참가 물질

4

반응물 2

HCID 1001PhenethylamineHCID 9765932-(2-Morpholinoethoxy)benzaldehyde

생성물 1

HCID 21322775N-[[2-[2-(4-Morpholinyl)ethoxy]phenyl]methylene]benzeneethanamine수율 85.6%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

2-[2-(4-Morpholinyl)ethoxy]benzaldehyde (55.9 g) is reacted with 29 g of phenethylamine in 240 ml of toluene following the procedure described in Example 1A to yield 68.8 g of product as an oil, boiling point 204°-210° C. at 0.1-0.2 mm of Hg.

출처 및 근거

ORD 기록
ord-4ac30af58cde4ba28f2ed7a5aea79b00
출처 데이터셋
uspto-grants-1979_04
특허 번호
US04151354

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