Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4-chlorophenol → 2-Acetylamino-4-chlorophenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4-chlorophenol | HCID 7265 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-Acetylamino-4-chlorophenol | HCID 95258 | 80.8% |
반응 단계
To a suspension of 2-amino-4-chlorophenol (1.43 g, 10.0 mmol) in methanol was added acetic anhydride (0.945 mL, 10.0 mmol) and the reaction mixture was stirred at room temperature for 2 h. The volatiles were removed in vacuo to give the subtitled compound (1.5 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07449475B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-40c22dff81724e1d9b69e1626f222a07 |
| 출처 메모 | uspto-grants-2008_11 |