Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl Salicylate → N-Methylsalicylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl Salicylate | HCID 4133 | — |
| 반응물 | Methylamine | HCID 6329 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | N-Methylsalicylamide | HCID 74624 | 90.6% |
반응 단계
A solution of methyl salicylate (5.16 mL, 40 mmol) in methanol (10 mL) was added dropwise to aqueous 40% methylamine (18.1 mL, 210 mmol) at 0° C. After addition was complete the reaction mixture was kept on stirring at room temperature overnight. The volatiles were removed in vacuo to give the subtitled compound (5.48 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07449475B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-6df448f464b946efb1c50dd83b17c1f4 |
| 출처 메모 | uspto-grants-2008_11 |