Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trifluoroacetic acid → Morpholin-2-ylmethyl trifluoroacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | tert-Butyl 2-(hydroxymethyl)morpholine-4-carboxylate | HCID 5201202 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Morpholin-2-ylmethyl trifluoroacetate | HCID 11206644 | — |
반응 단계
Tert-Butyl 2-(hydroxymethyl)-4-morpholinecarboxylate (5.13 g, 23.61 mmol) was treated with CF3CO2H (20 mL) in CH2Cl2 (50 mL) at room temperature for 3 h. The volatiles were removed in vacuo to give the subtitled compound (7.6 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07449475B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-cd13a1f2c918407faf5b11bd981b00ae |
| 출처 메모 | uspto-grants-2008_11 |