N-(2-Methoxyethyl)ethylamine → HCID 22313889, 화합물

HRID 270260

반응식

HRID 270260 반응식
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][C:15]([O:17][CH2:18][CH2:19][CH2:20]Br)=[CH:16][C:11]=3[S:10][N:9]=2)=[CH:4][CH:3]=1.[CH3:22][O:23][CH2:24][CH2:25][NH:26][CH2:27][CH3:28]>>[BrH:1].[Br:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][C:15]([O:17][CH2:18][CH2:19][CH2:20][N:26]([CH2:27][CH3:28])[CH2:25][CH2:24][O:23][CH3:22])=[CH:16][C:11]=3[S:10][N:9]=2)=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 546877N-(2-Methoxyethyl)ethylamineHCID 22314069HCID 22314069, 화합물

생성물 1

HCID 22313889HCID 22313889, 화합물

실험 절차

In analogy to example 3.1, 3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[d]isothiazole and N-(2-methoxyethyl)ethylamine were converted to yield (without extraction) [3-[3-(4-Bromo-phenyl)-benzo[d]isothiazol-6-yloxy]-propyl]-ethyl-(2-methoxy-ethyl)-amine hydrobromide as colorless oil, MS: 449(MH+, 1Br).

출처 및 근거

ORD 기록
ord-3531673cb1b746a4b5ef9085c445dbd7
출처 데이터셋
uspto-grants-2008_11
특허 번호
US07449483B2

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