Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boron trifluoride etherate → HCID 178505646, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boron trifluoride etherate | HCID 8000 | — |
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | Ethyl trifluoroacetate | HCID 9794 | — |
| 반응물 | 1-Ethynyl-3-fluorobenzene | HCID 520218 | — |
| 반응물 | Butyllithium | HCID 178418339 | — |
| 용매 | Benzene | HCID 241 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | HCID 178505646 | HCID 178505646 | — |
반응 단계
Following protocol H, 1-Ethynyl-3-fluoro-benzene was treated with n-BuLi, CF3CO2Et and BF3—OEt2 in THF. Reaction with hydrazine in benzene under similar reaction conditions yielded title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07449576B1 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-d8bdb191e76f452697277aaab9a78660 |
| 출처 메모 | uspto-grants-2008_11 |