2-[(Thiazol-2-yl)methylthio]ethylamine → HCID 178433298, 화합물

HRID 27096

반응식

HRID 27096 반응식
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2].[NH2:19][CH2:20][CH2:21][S:22][CH2:23][C:24]1[S:25][CH:26]=[CH:27][N:28]=1>C(#N)C>[N+:1]([CH:4]=[C:5]([NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])[NH:19][CH2:20][CH2:21][S:22][CH2:23][C:24]1[S:25][CH:26]=[CH:27][N:28]=1)([O-:3])=[O:2]

참가 물질

4

반응물 2

HCID 129234032-[(Thiazol-2-yl)methylthio]ethylamineHCID 178503826HCID 178503826, 화합물

생성물 1

HCID 178433298HCID 178433298, 화합물

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

Reaction of 1-nitro-2-methylthio-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene with an excess of 2-[(2-aminoethyl)thiomethyl]thiazole according to the procedure of Example 3, results in the production of 1-nitro-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene, m.p. 119°-120° (from acetonitrile).

출처 및 근거

ORD 기록
ord-b63e13f868df4715906ad7213e09b6c0
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04220652

연결된 노트

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