Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Bis(methylthio)-2-nitroethylene → 1-Nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| 반응물 | 2-(3-Aminopropyl)thiooxazole | HCID 20550119 | — |
| 생성물 | 1-Nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene | HCID 70541392 | 63% |
반응 단계
By the procedure of Example 8(i), 2-(3-aminopropylthio)oxazole (2.1 g) is reacted with 1-nitro-2,2-bis-methylthioethylene (2.0 g) to give 1-nitro-2-methylthio-2-[3-(2-oxazolylthio)propylamino]ethylene (2.1 g) which, on reaction with methylamine by the procedure of Example 8(ii) gives the title product (1.8 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220652 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-db6bb7fbc6ad4f9b830b4d94e9cb2908 |
| 출처 메모 | uspto-grants-1980_09 |