Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1-Bis(methylthio)-2-nitroethylene → 1-(Methylsulfanyl)-2-nitro-N-(2-{[(1,3-thiazol-2-yl)methyl]sulfanyl}ethyl)ethen-1-amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1-Bis(methylthio)-2-nitroethylene | HCID 83623 | — |
| 반응물 | 2-[(Thiazol-2-yl)methylthio]ethylamine | HCID 12923403 | — |
| 생성물 | 1-(Methylsulfanyl)-2-nitro-N-(2-{[(1,3-thiazol-2-yl)methyl]sulfanyl}ethyl)ethen-1-amine | HCID 70542948 | — |
반응 단계
By the procedure of Example 8(i), 2-[(2-aminoethyl)thiomethyl]thiazole (from the dihydrobromide, 4.0 g) is reacted with 1-nitro-2,2-bis methylthioethylene (2.0 g) to give 1-nitro-2-methylthio-2-[(2-thiazolylmethylthio)ethylamino]ethylene, m.p. 63°-64°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220652 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-007c2ea2f91c4a24a45bc31360407e67 |
| 출처 메모 | uspto-grants-1980_09 |