Ammonia → HCID 178433312, 화합물

HRID 27122

반응식

HRID 27122 반응식
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2].[NH3:19]>>[N+:1]([CH:4]=[C:5]([NH2:19])[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2]

참가 물질

3

반응물 2

HCID 222AmmoniaHCID 178503826HCID 178503826, 화합물

생성물 1

HCID 178433312HCID 178433312, 화합물

실험 절차

Reaction of 1-nitro-2-methylthio-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene (see Example 2(i)) with ammonia by the procedure of Example 2(ii) yields, after recrystallisation from methanol, the title compound, m.p. 193°-195° C.

후처리

  1. customyields
  2. customafter recrystallisation from methanol

출처 및 근거

ORD 기록
ord-9fa8f718586e4daca3c958f85e86d956
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04220652

연결된 노트

불러오는 중…