Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Itaconic Anhydride | HCID 75110 | — |
| 용매 | Methyl Chloride | HCID 6327 | — |
| 생성물 | 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid | HCID 21935560 | — |
반응 단계
A solution of 2-methylenesuccinic anhydride (500 mg, 4.46 mmol) and aniline (0.4 mL, 4.46 mmol) in CH3Cl were shaken overnight. A precipitate formed, which was filtered off, washed with hexanes, and dried under vacuum to afford 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07452889B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-682c33e9511d4681b3e6095fa4659f39 |
| 출처 메모 | uspto-grants-2008_11 |