Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → N-(((2,6-Dichlorophenyl)amino)thioxomethyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzyl Chloride | HCID 7503 | — |
| 반응물 | 2,6-Dichloroaniline | HCID 11846 | — |
| 반응물 | Ammonium thiocyanate | HCID 15666 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N-(((2,6-Dichlorophenyl)amino)thioxomethyl)benzamide | HCID 702451 | — |
반응 단계
To 51.8 g (0.68 mole) of ammonium thiocyanate in 300 ml acetone is added 86.8 g (0.62 mole) of benzyl chloride. The reaction mixture is refluxed for about 5 min. and then 100 g (0.62 mole) of 2,6-dichloroaniline in 200 ml acetone is added at a rate to maintain reflux. The mixture is refluxed for 11/2 hours, cooled, poured into 11/2 liters of ice and water, filtered to obtain 1-(2,6-dichlorophenyl)-3-benzoylthiourea.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220658 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-ee423d099bfc46fcb321850ee7ca0ec7 |
| 출처 메모 | uspto-grants-1980_09 |