(Pyridin-4-yl)boronic acid → 3-(4-Chloro-2-methoxybenzyl)pyridine
반응식
O1CCCOB1[C:7]1[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=1.Br[CH2:14][C:15]1[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=1[O:22][CH3:23].N1C=CC(B(O)O)=CC=1>>[Cl:21][C:18]1[CH:19]=[CH:20][C:15]([CH2:14][C:7]2[CH:8]=[N:9][CH:10]=[CH:11][CH:12]=2)=[C:16]([O:22][CH3:23])[CH:17]=1참가 물질
4
실험 절차
The title compound was prepared by substituting 1-bromomethyl-4-chloro-2-methoxy-benzene and 3-[1,3,2]dioxaborinan-2-yl-pyridine for 1-bromomethyl-4-chloro-2-methoxy-benzene and 4-pyridyl boronic acid, respectively, in Example 700A. MS (ESI) m/e 234 (M+H)+.
출처 및 근거
- ORD 기록
- ord-8d235e009903405580d4e96f80d40714
- 출처 데이터셋
- uspto-grants-2008_11
- 특허 번호
- US07456169B2
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