Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-Ethylcyclobutanecarboxylic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Cyclobutanecarboxylic acid, 3-ethyl- | HCID 47796 | — |
| 생성물 | 3-Ethylcyclobutanecarboxylic acid chloride | HCID 45081271 | 60.6% |
반응 단계
A mixture of 3.3 g (0.027 mole) of 3-ethylcyclobutanecarboxylic acid (prepared in 1E) and 9.4 g (5.7 ml, 0.080 mole) of thionyl chloride was prepared and allowed to stir at room temperature for about 15 hr. Excess thionyl chloride was removed by distillation at atmospheric pressure. The residue was distilled at reduced pressure to yield 2.4 g of the title compound having the following physical characteristics:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220795 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-bd5aa059603b4de884c3fae56ebe28c3 |
| 출처 메모 | uspto-grants-1980_09 |