Acetone → 9-Hydroxynonan-2-one

HRID 27312

반응식

HRID 27312 반응식
[OH2:1].[C:2]1([CH3:12])[CH:7]=[CH:6][C:5](S(O)(=O)=O)=[CH:4][CH:3]=1.[CH3:13][C:14](C)=[O:15]>>[O:1]=[C:2]([CH3:12])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:13][CH2:14][OH:15]

참가 물질

3

반응물 2

HCID 180AcetoneHCID 521998p-Toluenesulfonic acid monohydrate

생성물 1

HCID 5374089-Hydroxynonan-2-one

실험 절차

A solution containing 56.6 g of 8-oxononan-1-ol ethylene ketol (prepared in Example 22 B-5) in 210 ml acetone and 50 mg p-toluenesulfonic acid monohydrate was stirred at room temperature for about 15 to 17 hr. The acetone was removed in vacuo to yield the title compound having the following physical characteristics:

후처리

  1. customThe acetone was removed in vacuo

출처 및 근거

ORD 기록
ord-693e33c552514efd8070df5fd9ba4b0a
출처 데이터셋
uspto-grants-1980_09
특허 번호
US04220795

연결된 노트

불러오는 중…