Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Acifluorfen sodium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Acifluorfen | HCID 44073 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Acifluorfen sodium | HCID 44072 | 105.4% |
반응 단계
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (1.7 g, 0.0047 mole) is dissolved in methanol (25 ml) and sodium hydroxide (4.7 ml of 1 N NaOH in methanol, 0.0047 mole) is added rapidly. The solvent is then removed in vacuo to give 1.9 g of product that decomposes at 217° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220468 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-f721db82d1d0420393e4aedde7b519cb |
| 출처 메모 | uspto-grants-1980_09 |