Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylamine → Dicyclohexylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylamine | HCID 7582 | — |
| 반응물 | Acifluorfen | HCID 44073 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | Dicyclohexylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate | HCID 21280067 | 59.9% |
반응 단계
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (3.0 g, 0.0083 mole) is dissolved in glyme (20 ml) and dicyclohexylamine (1.64 g, 0.0091 mole) is added at room temperature while stirring. The solvent is removed in vacuo, the residue triturated with petroleum ether (bp 30°-60° C.) and dried to give 2.7 g of product, mp 197°-9° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220468 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-599cb009560b44358f78e2c375a9f8ee |
| 출처 메모 | uspto-grants-1980_09 |