Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acifluorfen → t-Octylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acifluorfen | HCID 44073 | — |
| 반응물 | tert-Octylamine | HCID 61017 | — |
| 용매 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 생성물 | t-Octylammonium 5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate | HCID 21280025 | 68.7% |
반응 단계
5-(2-Chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (3.0 g, 0.0083 mole) is dissolved in glyme (20 ml) and t-octylamine (1.17 g, 0.0091 mole) is added rapidly while stirring. The solvent is removed in vacuo and the residue triturated with petroleum either (bp 30°-60° C.) and dried to give 2.8 g of product, mp 140°-57° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04220468 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-884dca2509ea4a878eebbc80f47f85a6 |
| 출처 메모 | uspto-grants-1980_09 |