Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 2-pyridinecarboxylate → 1,5-Bis(4-ethoxy-pyridin-2-yl)pentane-1,3,5-trione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 2-pyridinecarboxylate | HCID 17307 | — |
| 반응물 | Ethyl 4-ethoxypicolinate | HCID 49853411 | — |
| 생성물 | 1,5-Bis(4-ethoxy-pyridin-2-yl)pentane-1,3,5-trione | HCID 17971932 | — |
반응 단계
This compound is prepared in a manner analogous to that described in Example 1, Step 1, for pyridine-2-carboxylic acid ethyl ester, but instead 4-ethoxy-pyridine-2-carboxylic acid ethyl ester from Example 17 is used. The yellowish crude product is used for further syntheses without special purification steps. IR (cm−1): 1557 (vs); 1469 (w); 1436 (w); 1300 (m); 1207 (m); 1186 (m); 1035 (m); 818 (m).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07456285B2 |
| 출처 데이터셋 | uspto-grants-2008_11 |
| ORD ID | ord-fcfd0baf446f430c93ca8c16ecd91c11 |
| 출처 메모 | uspto-grants-2008_11 |