Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propargylamine → HCID 178457492, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propargylamine | HCID 239041 | — |
| 반응물 | Benzene, [[2,2-bis(methylthio)ethenyl]sulfonyl]- | HCID 12296879 | — |
| 반응물 | HCID 178433288 | HCID 178433288 | — |
| 반응물 | HCID 178503846 | HCID 178503846 | — |
| 생성물 | HCID 178457492 | HCID 178457492 | — |
반응 단계
Reaction of methylphenylsulfone with carbon disulphide under strongly basic conditions and treatment of the product with methyl iodide yields 1-benzenesulphonyl-2,2-bis(methylthio)ethylene. When 1-benzenesulfonyl-2,2-bis(methylthio)ethylene is reacted with 2-[(4-methyl-1H-imidazol-5-yl)-methylthio]ethylamine according to the procedure of Example 6, Step A, the product is 1-benzenesulfonyl-2-methylthio-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene. Reaction of this methylthio compound with propargylamine by the procedure of Example 6, Step B, yields the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04221737 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-a859d5e12e754679aba9805f030eea4e |
| 출처 메모 | uspto-grants-1980_09 |