4-(Hydroxymethyl)benzaldehyde → 4-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde

HRID 274037

반응식

HRID 274037 반응식
[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8](Cl)=[O:9])([CH3:4])([CH3:3])[CH3:2].[OH:16][CH2:17][C:18]1[CH:25]=[CH:24][C:21]([CH:22]=[O:23])=[CH:20][CH:19]=1>>[C:1]([C:5]1[CH:6]=[C:7]([CH:11]=[CH:12][C:13]=1[O:14][CH3:15])[C:8]([O:23][CH2:22][C:21]1[CH:24]=[CH:25][C:18]([CH:17]=[O:16])=[CH:19][CH:20]=1)=[O:9])([CH3:4])([CH3:3])[CH3:2]

참가 물질

3

반응물 2

HCID 5563304-(Hydroxymethyl)benzaldehydeHCID 136335553-Tert-butyl-4-methoxybenzoyl chloride

생성물 1

HCID 214745254-(3-tert-Butyl-4-methoxybenzoyloxymethyl)benzaldehyde

실험 절차

In a manner similar to Example 1(d), by reaction of 7.6 g (34 mmol) of 3-tert-butyl-4-methoxybenzoyl chloride with 4.6 g (34 mmol) of 4-hydroxymethylbenzaldehyde, 5.6 g (51%) of the expected aldehyde, melting point 75°-6° C., are obtained.

후처리

  1. customare obtained

출처 및 근거

ORD 기록
ord-ed07a39e5049450bace6f0c1deaed411
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05387594

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