반응식
[NH2:1][N:2]1[CH2:8][CH2:7][C:6]2[CH:9]=[CH:10][CH:11]=[CH:12][C:5]=2[CH2:4][CH2:3]1.C([N:16]1[CH2:20][CH2:19][NH:18][C:17]1=O)(=O)C>>[NH:18]1[CH2:19][CH2:20][N:16]=[C:17]1[NH:1][N:2]1[CH2:3][CH2:4][C:5]2[CH:12]=[CH:11][CH:10]=[CH:9][C:6]=2[CH2:7][CH2:8]1참가 물질
3
실험 절차
5 g of (0.03 M) 3-amino-2,3,4,5-tetrahydro-1H-3-benzazepin and 4.3 g of (0.034 M) 1-acetyl-imidazolidin-2-one are stirred in 50 ml POCL3 for 1 hour at 100° C. The remaining process steps are analogous to those set forth in Example 5.
출처 및 근거
- ORD 기록
- ord-ca09b85885634a7d906c54626f6893d9
- 출처 데이터셋
- uspto-grants-1980_09
- 특허 번호
- US04221798
연결된 노트
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