참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | Allyltriphenylphosphonium bromide | HCID 197740 | — |
반응 단계
86.7 parts of triphenylphosphine was dissolved in 200 parts of xylene and 40.0 parts of allyl bromide was added thereto. The mixture was gradually heated and allowed to react at 134° C. for 3 hr. After the mixture was cooled to 30° C., the resulting colorless crystals were collected by filtration and washed with toluene to obtain 122.7 parts of allyltriphenylphosphonium bromide (compound No. 16).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05389486 |
|---|
| 출처 데이터셋 | uspto-grants-1995_02 |
|---|
| ORD ID | ord-7ebd87c006504dd293d5a25acc3a52f1 |
|---|
| 출처 메모 | uspto-grants-1995_02 |
|---|
