참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | Benzene, (3-chloro-1-propenyl)- | HCID 94242 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | [(E)-cinnamyl]-triphenyl-phosphonium chloride | HCID 73729 | — |
반응 단계
88.2 parts of triphenylphosphine was dissolved in 240 parts of xylene and 51.3 parts of cinnamyl chloride was added thereto. The mixture was heated at 130° C. for 4 hr. After the mixture was cooled to 30° C., the resulting colorless crystals were collected by filtration and washed with toluene to obtain 117.4 parts of cinnamyltriphenylphosphonium chloride (compound No. 15).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05389486 |
|---|
| 출처 데이터셋 | uspto-grants-1995_02 |
|---|
| ORD ID | ord-fa939c3d200942e0a4f0c4e26a59ee5a |
|---|
| 출처 메모 | uspto-grants-1995_02 |
|---|
