Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine → 2-[(4-Chlorophenyl)methyl]azepane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine | HCID 23342815 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 생성물 | 2-[(4-Chlorophenyl)methyl]azepane | HCID 3933809 | — |
반응 단계
Hydrogenate the thus-obtained 2-(4-chlorobenzyl)-4,5,6,7-tetrahydro-3H-azepine with platinum/active carbon/ hydrogen. Filter out the catalyst, concentrate the filtrate and distil to obtain 61.9 g (68% of theory) of the title compound with a BP of 93° at 0.1 mm of Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04221788 |
| 출처 데이터셋 | uspto-grants-1980_09 |
| ORD ID | ord-a9a8a7247d0e458c9769f6464a652878 |
| 출처 메모 | uspto-grants-1980_09 |