6-Hydroxy-5,5-diethyl-1-hexanesulfonamide → 1-Heptanesulfonamide, 5-ethyl-5-((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-

HRID 274272

반응식

HRID 274272 반응식
[OH:1][CH2:2][C:3]([CH2:14][CH3:15])([CH2:12][CH3:13])[CH2:4][CH2:5][CH2:6][CH2:7][S:8]([NH2:11])(=[O:10])=[O:9].Cl[C:17]1[C:18]([CH3:26])=[CH:19][C:20]2[N:21]([N:23]=[CH:24][N:25]=2)[N:22]=1>>[CH2:12]([C:3]([CH2:14][CH3:15])([CH2:4][CH2:5][CH2:6][CH2:7][S:8](=[O:9])(=[O:10])[NH2:11])[CH2:2][O:1][C:17]1[C:18]([CH3:26])=[CH:19][C:20]2[N:21]([N:23]=[CH:24][N:25]=2)[N:22]=1)[CH3:13]

참가 물질

3

반응물 2

HCID 106575306-Hydroxy-5,5-diethyl-1-hexanesulfonamideHCID 118051586-Chloro-7-methyl-[1,2,4]triazolo[1,5-b]pyridazine

생성물 1

HCID 30737901-Heptanesulfonamide, 5-ethyl-5-((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-

실험 절차

Using 6-hydroxy-5,5-diethyl-1-hexanesulfonamide and 6-chloro-7-methyl[1,2,4]triazolo[1,5-b]pyridazine, the same reaction was conducted as in Example 5 to produce the title compound. m.p. 132°-133° C.

후처리

  1. customthe same reaction

출처 및 근거

ORD 기록
ord-31fc2eefdb594f198f1f9e3aef219c49
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05389633

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