5-Hydroxy-4,4-diethyl-1-pentanesulfonamide → Hexanesulfonamide, 4-ethyl-4-(((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-

HRID 274273

반응식

HRID 274273 반응식
[OH:1][CH2:2][C:3]([CH2:13][CH3:14])([CH2:11][CH3:12])[CH2:4][CH2:5][CH2:6][S:7]([NH2:10])(=[O:9])=[O:8].Cl[C:16]1[C:17]([CH3:25])=[CH:18][C:19]2[N:20]([N:22]=[CH:23][N:24]=2)[N:21]=1>>[CH2:13]([C:3]([CH2:11][CH3:12])([CH2:4][CH2:5][CH2:6][S:7](=[O:8])(=[O:9])[NH2:10])[CH2:2][O:1][C:16]1[C:17]([CH3:25])=[CH:18][C:19]2[N:20]([N:22]=[CH:23][N:24]=2)[N:21]=1)[CH3:14]

참가 물질

3

반응물 2

HCID 107278035-Hydroxy-4,4-diethyl-1-pentanesulfonamideHCID 118051586-Chloro-7-methyl-[1,2,4]triazolo[1,5-b]pyridazine

생성물 1

HCID 3073791Hexanesulfonamide, 4-ethyl-4-(((7-methyl(1,2,4)triazolo(1,5-b)pyridazin-6-yl)oxy)methyl)-

실험 절차

Using 5-hydroxy-4,4-diethyl-1-pentanesulfonamide and 6-chloro-7-methyl[1,2,4]triazolo[1,5-b]pyridazine, the same reaction was conducted as in Example 5 to produce the title compound. m.p. 157°-158° C.

후처리

  1. customthe same reaction

출처 및 근거

ORD 기록
ord-e8862145a77d46539cd788b09b3cbb16
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05389633

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