참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3,4-Diaminopyridine | HCID 5918 | — |
| 반응물 | Pentanoic Acid | HCID 7991 | — |
| 생성물 | HCID 178441556 | HCID 178441556 | 99.6% |
반응 단계
A mixture of 3 g of 3,4-diamino-pyridine and 8.28 g of valeric acid was heated to 70° C. for 18 hours and the reaction medium was chromatographed on silica (eluant: ethyl acetatemethanol (8-2)) to obtain 4.8 g of the expected product which was used as is for the following step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05389634 |
|---|
| 출처 데이터셋 | uspto-grants-1995_02 |
|---|
| ORD ID | ord-ad0e57e92b4348ebbe384289d16ea0c2 |
|---|
| 출처 메모 | uspto-grants-1995_02 |
|---|
