Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → HCID 15239119, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | HCID 15239125 | HCID 15239125 | — |
| 반응물 | HCID 178527880 | HCID 178527880 | — |
| 생성물 | HCID 15239119 | HCID 15239119 | — |
반응 단계
Generally following the procedure of Example 7, 2-mercapto-2-thiazoline (0.67 g, 5.6 mmol) is treated with sodium hydride (0.35 g, 7.3 mmol), with cooling, and the resulting sodium salt is reacted with 1-methyl-2-[4-(1methylpropylthio)phenoxy]ethyl bromide (1.70 g, 5.6 mmol) at RT to give 2-{1-methyl-2-[4-(1-methylpropylthio)phenoxy]ethylthio}-2-thiazoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05389651 |
| 출처 데이터셋 | uspto-grants-1995_02 |
| ORD ID | ord-e8df4daf53eb4aa58097930efe075e3b |
| 출처 메모 | uspto-grants-1995_02 |