Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-4-(4-nitrophenoxy)benzene → 4-(4-Chlorophenoxy)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-4-(4-nitrophenoxy)benzene | HCID 15786 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-(4-Chlorophenoxy)aniline | HCID 7578 | 99.3% |
반응 단계
A suspension of 16.0 g (64.1 mmole) of 4-(4'-chlorophenoxy) nitrobenzene and 75% Pt, 161 mg of platinum oxide (641 μmole, 1 mole %) in 200 ml of ethanol was stirred vigorously under hydrogen until hydrogen uptake ceased (about 4 hours). The suspension was filtered through celite and the solution was evaporated to dryness to obtain 13.94 g (99.3%) of the desired product as a pale brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05389652 |
| 출처 데이터셋 | uspto-grants-1995_02 |
| ORD ID | ord-06bcff59bd4a47bd9898ddf5c335cb0b |
| 출처 메모 | uspto-grants-1995_02 |