Sulfuric Acid → alpha,2,6-Trimethylmorpholin-4-ylethanol

HRID 274990

반응식

HRID 274990 반응식
[OH:1][CH:2]([CH3:13])[CH2:3][N:4]([CH2:9][CH:10]([OH:12])[CH3:11])[CH2:5][CH:6](O)[CH3:7].S(=O)(=O)(O)O>>[OH:1][CH:2]([CH3:13])[CH2:3][N:4]1[CH2:9][CH:10]([CH3:11])[O:12][CH:6]([CH3:7])[CH2:5]1

참가 물질

3

반응물 2

HCID 1118Sulfuric AcidHCID 24730Triisopropanolamine

생성물 1

HCID 98999alpha,2,6-Trimethylmorpholin-4-ylethanol

실험 절차

3 g of tris-(2-hydroxypropyl)amine and 1 g of SnO2 doped with sulfuric acid were heated in a manner similar to that described in Example 3 for a period of 1 h at 250° C. There were obtained, in addition to 50 wt % of educt, 30 wt % of N-(2-hydroxypropyl)-2,6-dimethylmorpholine.

후처리

  1. temperaturewere heated in a manner similar to

출처 및 근거

ORD 기록
ord-b688cab9275c4fb6885fb2fc7cb74e14
출처 데이터셋
uspto-grants-1995_02
특허 번호
US05391734

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