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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 275279생성일: 2026년 10월 27일

4-Pyridinecarboxylic acid, 1-oxide → 6,11-dihydro-11-(4-piperidinylidene)-5H-imidazo[2,1-b][3]benzazepine

https://huagongshe.com/reaction/275279

반응식

참여 물질

역할이름HCID투입량
반응물4-Pyridinecarboxylic acid, 1-oxideHCID 26130—
반응물1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochlorideHCID 2723939—
반응물1-Hydroxybenzotriazole hydrateHCID 2796029—
생성물6,11-dihydro-11-(4-piperidinylidene)-5H-imidazo[2,1-b][3]benzazepineHCID 18612492—

반응 단계

6,11-dihydro-11-(4-piperidinylidene)-5H-imidazo[2,1-b][3]benzazepine (C) was prepared as described in Example 4. The Aldrich Chemical Company supplies 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, pyridine-4-carboxylic acid N-oxide, and 1-hydroxybenzotriazole hydrate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05393753
출처 데이터셋uspto-grants-1995_02
ORD IDord-ade618fc01a642c6b8c4f20c8512cbc5
출처 메모uspto-grants-1995_02