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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 275787생성일: 2026년 10월 27일

6-Nitro-o-anisidine → 3-Methoxybenzene-1,2-diamine

https://huagongshe.com/reaction/275787

반응식

참여 물질

역할이름HCID투입량
반응물6-Nitro-o-anisidineHCID 85491—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물3-Methoxybenzene-1,2-diamineHCID 184268101.9%

반응 단계

2-Amino-3-nitroanisole (4.3 g) was hydrogenated in ethyl acetate (200 ml) using catalytic 10% palladium on charcoal under an atmosphere of hydrogen at ambient temperature. Once complete the reaction mixture was filtered through Celite and the filtrate evaporated in vacuo to afford the title compound as a brown liquid (3.60 g).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06353010B1
출처 데이터셋uspto-grants-2002_03
ORD IDord-1931361c855c4e49b5bf142cad92b2bd
출처 메모uspto-grants-2002_03