Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Nitro-o-anisidine → 3-Methoxybenzene-1,2-diamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Nitro-o-anisidine | HCID 85491 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 3-Methoxybenzene-1,2-diamine | HCID 184268 | 101.9% |
반응 단계
2-Amino-3-nitroanisole (4.3 g) was hydrogenated in ethyl acetate (200 ml) using catalytic 10% palladium on charcoal under an atmosphere of hydrogen at ambient temperature. Once complete the reaction mixture was filtered through Celite and the filtrate evaporated in vacuo to afford the title compound as a brown liquid (3.60 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06353010B1 |
| 출처 데이터셋 | uspto-grants-2002_03 |
| ORD ID | ord-1931361c855c4e49b5bf142cad92b2bd |
| 출처 메모 | uspto-grants-2002_03 |