참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Ethyl orthopropionate | HCID 66995 | — |
| 반응물 | 1,3-Benzenediol, 2-amino-, hydrochloride (1:1) | HCID 459247 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Ethylbenzo[d]oxazol-4-ol | HCID 15665680 | — |
반응 단계
A mixture of 2-aminoresorcinol hydrochloride (5.0 g) and triethylorthopropionate (13.7 ml) was heated to 150° C. for 2 h before being poured into a mixture of water (140 ml) and ethanol (35 ml). The mixture was stirred vigorously for 30 minutes at room temperature. The resulting precipitate was removed by filtration and dried to give the title compound as a beige solid (4.11 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06353010B1 |
|---|
| 출처 데이터셋 | uspto-grants-2002_03 |
|---|
| ORD ID | ord-431cdd863f2841b39b43c21f7b1cdf97 |
|---|
| 출처 메모 | uspto-grants-2002_03 |
|---|
